Information card for entry 7707616

Structure parameters

• Formula: C48 H92 Ge2 N4 Si4
• Calculated formula: C48 H92 Ge2 N4 Si4
• Title of publication: Bulky arene-bridged bis(amide) and bis(amidinate) complexes of germanium(II) and tin(II).
• Authors of publication: Garg, Palak; Dange, Deepak; Jones, Cameron
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 26
• Pages of publication: 9118 - 9122
• a: 14.8934 ± 0.0007 Å
• b: 9.6017 ± 0.0004 Å
• c: 18.8362 ± 0.0008 Å
• α: 90°
• β: 96.359 ± 0.004°
• γ: 90°
• Cell volume: 2677 ± 0.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0742
• Residual factor for significantly intense reflections: 0.0553
• Weighted residual factors for significantly intense reflections: 0.1391
• Weighted residual factors for all reflections included in the refinement: 0.1504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No