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Information card for entry 7707772
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Coordinates | 7707772.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C16 H18 Al Br O |
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Calculated formula | C16 H18 Al Br O |
Title of publication | Synthesis, structure and insertion reactivity of Lewis acidic 9-aluminafluorenes. |
Authors of publication | Drescher, Regina; Wüst, Leonie; Mihm, Cornelius; Krummenacher, Ivo; Hofmann, Alexander; Goettel, James; Braunschweig, Holger |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2021 |
Journal volume | 50 |
Journal issue | 30 |
Pages of publication | 10400 - 10404 |
a | 25.3861 ± 0.0008 Å |
b | 7.1604 ± 0.0003 Å |
c | 18.1719 ± 0.0006 Å |
α | 90° |
β | 108.642 ± 0.001° |
γ | 90° |
Cell volume | 3129.89 ± 0.19 Å3 |
Cell temperature | 105 ± 2 K |
Ambient diffraction temperature | 105 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0653 |
Residual factor for significantly intense reflections | 0.0557 |
Weighted residual factors for significantly intense reflections | 0.1314 |
Weighted residual factors for all reflections included in the refinement | 0.1382 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.089 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7707772.html
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