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Information card for entry 7707777
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Coordinates | 7707777.cif |
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Original paper (by DOI) | HTML |
Formula | C21 H24 Al Br N2 |
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Calculated formula | C21 H24 Al Br N2 |
Title of publication | Synthesis, structure and insertion reactivity of Lewis acidic 9-aluminafluorenes. |
Authors of publication | Drescher, Regina; Wüst, Leonie; Mihm, Cornelius; Krummenacher, Ivo; Hofmann, Alexander; Goettel, James; Braunschweig, Holger |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2021 |
Journal volume | 50 |
Journal issue | 30 |
Pages of publication | 10400 - 10404 |
a | 8.3702 ± 0.0002 Å |
b | 23.2949 ± 0.0006 Å |
c | 20.455 ± 0.0005 Å |
α | 90° |
β | 98.189 ± 0.001° |
γ | 90° |
Cell volume | 3947.71 ± 0.17 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0389 |
Residual factor for significantly intense reflections | 0.0318 |
Weighted residual factors for significantly intense reflections | 0.0787 |
Weighted residual factors for all reflections included in the refinement | 0.0823 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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