Information card for entry 7707836

Structure parameters

• Formula: C48 H84 Co4 Ge O12 P4
• Calculated formula: C48 H84 Co4 Ge O12 P4
• Title of publication: GeCl_x[Co(CO)₃PR₃]_4-x (x = 0-3; R = ⁿPr, ⁿBu): from cobalt substituted germanes to novel binary cluster compounds.
• Authors of publication: Preißing, Lars; Behling, Elias; Schnepf, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 31
• Pages of publication: 10789 - 10797
• a: 28.9936 ± 0.0006 Å
• b: 28.9936 ± 0.0006 Å
• c: 28.9936 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 24372.9 ± 0.9 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150.01 K
• Number of distinct elements: 6
• Space group number: 198
• Hermann-Mauguin space group symbol: P 21 3
• Hall space group symbol: P 2ac 2ab 3
• Residual factor for all reflections: 0.0831
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1214
• Weighted residual factors for all reflections included in the refinement: 0.137
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No