Information card for entry 7707841

Structure parameters

• Formula: C24 H42 Cl2 Co2 Ge O6 P2
• Calculated formula: C24 H42 Cl2 Co2 Ge O6 P2
• Title of publication: GeCl_x[Co(CO)₃PR₃]_4-x (x = 0-3; R = ⁿPr, ⁿBu): from cobalt substituted germanes to novel binary cluster compounds.
• Authors of publication: Preißing, Lars; Behling, Elias; Schnepf, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 31
• Pages of publication: 10789 - 10797
• a: 10.8319 ± 0.0015 Å
• b: 18.047 ± 0.002 Å
• c: 17.997 ± 0.002 Å
• α: 90°
• β: 101.607 ± 0.002°
• γ: 90°
• Cell volume: 3446.2 ± 0.7 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150.01 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0545
• Residual factor for significantly intense reflections: 0.0344
• Weighted residual factors for significantly intense reflections: 0.0755
• Weighted residual factors for all reflections included in the refinement: 0.0851
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No