Information card for entry 7707937

Structure parameters

• Formula: B2 O25 Pb6 Si8
• Calculated formula: B2.036 O25 Pb6 Si7.964
• Title of publication: High-temperature, high-pressure hydrothermal synthesis, crystal structure, and solid state NMR spectroscopy of a lead borosilicate with boron-silicon mixing: Pb₆B₂Si₈O₂₅.
• Authors of publication: Chang, Ling-Wei; Lii, Kwang-Hwa
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 32
• Pages of publication: 11173 - 11179
• a: 9.509 ± 0.0002 Å
• b: 9.509 ± 0.0002 Å
• c: 42.3552 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3316.71 ± 0.12 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 167
• Hermann-Mauguin space group symbol: R -3 c :H
• Hall space group symbol: -R 3 2"c
• Residual factor for all reflections: 0.0183
• Residual factor for significantly intense reflections: 0.0147
• Weighted residual factors for significantly intense reflections: 0.0301
• Weighted residual factors for all reflections included in the refinement: 0.0309
• Goodness-of-fit parameter for all reflections included in the refinement: 1.126
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No