Information card for entry 7707958

Structure parameters

• Common name: Pr(Ph-PDB)3
• Chemical name: Pr2(BH3Ph2BH3)6
• Formula: C72 H96 B12 P6 Pr2
• Calculated formula: C72 H96 B12 P6 Pr2
• Title of publication: Mechanochemical synthesis and structural analysis of trivalent lanthanide and uranium diphenylphosphinodiboranates.
• Authors of publication: Fetrow, Taylor V.; Daly, Scott R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 33
• Pages of publication: 11472 - 11484
• a: 37.239 ± 0.004 Å
• b: 9.6296 ± 0.001 Å
• c: 23.924 ± 0.002 Å
• α: 90°
• β: 107.636 ± 0.005°
• γ: 90°
• Cell volume: 8175.9 ± 1.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1154
• Residual factor for significantly intense reflections: 0.0575
• Weighted residual factors for significantly intense reflections: 0.1023
• Weighted residual factors for all reflections included in the refinement: 0.124
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No