Information card for entry 7708035

Structure parameters

• Formula: C20 H10 O8 Se2 W2
• Calculated formula: C20 H10 O8 Se2 W2
• Title of publication: Reactivity of the pentelidene complexes [Cp*E{W(CO)₅}₂] (E = P, As) towards dichalcogenides and chalcogenols - synthesis of novel chalcogenopentelidene complexes.
• Authors of publication: Rummel, Lena; Lassandro, Giuliano; Seidl, Michael; Timoshkin, Alexey Y.; Scheer, Manfred
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 36
• Pages of publication: 12648 - 12654
• a: 18.3332 ± 0.0005 Å
• b: 7.206 ± 0.0002 Å
• c: 17.1601 ± 0.0005 Å
• α: 90°
• β: 102.976 ± 0.004°
• γ: 90°
• Cell volume: 2209.11 ± 0.11 ų
• Cell temperature: 123 ± 0.14 K
• Ambient diffraction temperature: 123 ± 0.14 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0392
• Residual factor for significantly intense reflections: 0.0351
• Weighted residual factors for significantly intense reflections: 0.0978
• Weighted residual factors for all reflections included in the refinement: 0.1019
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No