Information card for entry 7708037

Structure parameters

• Formula: C23 H22 O5 Te2 W
• Calculated formula: C23 H22 O5 Te2 W
• Title of publication: Reactivity of the pentelidene complexes [Cp*E{W(CO)₅}₂] (E = P, As) towards dichalcogenides and chalcogenols - synthesis of novel chalcogenopentelidene complexes.
• Authors of publication: Rummel, Lena; Lassandro, Giuliano; Seidl, Michael; Timoshkin, Alexey Y.; Scheer, Manfred
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 36
• Pages of publication: 12648 - 12654
• a: 16.5396 ± 0.0012 Å
• b: 18.58 ± 0.0003 Å
• c: 28.924 ± 0.002 Å
• α: 90°
• β: 145.249 ± 0.017°
• γ: 90°
• Cell volume: 5067 ± 2 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 ± 1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0337
• Residual factor for significantly intense reflections: 0.0296
• Weighted residual factors for significantly intense reflections: 0.0756
• Weighted residual factors for all reflections included in the refinement: 0.0776
• Goodness-of-fit parameter for all reflections included in the refinement: 1.097
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No