Crystallography Open Database

Information card for entry 7708094

Preview

Coordinates	7708094.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H58 Ga0.6 K0.4 N3
Calculated formula	C46 H58 Ga0.61 K0.39 N3
Title of publication	A bis(imino)carbazolate pincer ligand stabilized mononuclear gallium(I) compound: synthesis, characterization, and reactivity.
Authors of publication	Li, Hao; He, Yuhao; Liu, Chunmeng; Tan, Gengwen
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	36
Pages of publication	12674 - 12680
a	12.4878 ± 0.0007 Å
b	11.683 ± 0.0006 Å
c	28.9149 ± 0.0015 Å
α	90°
β	99.338 ± 0.002°
γ	90°
Cell volume	4162.6 ± 0.4 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1179
Residual factor for significantly intense reflections	0.0716
Weighted residual factors for significantly intense reflections	0.1701
Weighted residual factors for all reflections included in the refinement	0.1876
Goodness-of-fit parameter for all reflections included in the refinement	1.078
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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