Information card for entry 7708182

Structure parameters

• Formula: C88 H146 B8 Li6 N8 O18
• Calculated formula: C88 H146 B8 Li6 N8 O18
• Title of publication: N-H deprotonation of a diaminodialkoxido diborane(4) - a structural study on bifunctional Lewis acids/bases and their dimerisation to B(sp²)₂B(sp³)₂N₂ six membered rings.
• Authors of publication: Drescher, Wiebke; Kleeberg, Christian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 37
• Pages of publication: 13149 - 13157
• a: 27.2197 ± 0.0008 Å
• b: 12.9528 ± 0.0005 Å
• c: 33.2002 ± 0.0012 Å
• α: 90°
• β: 103.948 ± 0.003°
• γ: 90°
• Cell volume: 11360.3 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0684
• Residual factor for significantly intense reflections: 0.0578
• Weighted residual factors for significantly intense reflections: 0.152
• Weighted residual factors for all reflections included in the refinement: 0.1602
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No