Information card for entry 7708186

Structure parameters

• Formula: C63.24 H112.48 B4 Li6 N4 O11.81
• Calculated formula: C63.24 H112.48 B4 Li6 N4 O11.81
• Title of publication: N-H deprotonation of a diaminodialkoxido diborane(4) - a structural study on bifunctional Lewis acids/bases and their dimerisation to B(sp²)₂B(sp³)₂N₂ six membered rings.
• Authors of publication: Drescher, Wiebke; Kleeberg, Christian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 37
• Pages of publication: 13149 - 13157
• a: 22.5108 ± 0.0004 Å
• b: 12.8635 ± 0.0002 Å
• c: 27.2387 ± 0.0005 Å
• α: 90°
• β: 111.665 ± 0.002°
• γ: 90°
• Cell volume: 7330.3 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.1607
• Weighted residual factors for all reflections included in the refinement: 0.1655
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No