Information card for entry 7708198

Structure parameters

• Formula: C34 H27 N O
• Calculated formula: C34 H27 N O
• Title of publication: On the edge of the steric repulsion and reactivity of bulky anilines; a case study of chloro(imino)phosphine synthesis
• Authors of publication: Vrána, Jan; Němec, Vlastimil; Samsonov, Maksim Andreevich; Růžička, Aleš
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 5.4624 ± 0.0011 Å
• b: 13.41 ± 0.003 Å
• c: 17.986 ± 0.004 Å
• α: 102.708 ± 0.011°
• β: 97.662 ± 0.012°
• γ: 98.134 ± 0.011°
• Cell volume: 1253.7 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1486
• Residual factor for significantly intense reflections: 0.1089
• Weighted residual factors for significantly intense reflections: 0.2763
• Weighted residual factors for all reflections included in the refinement: 0.2953
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No