Information card for entry 7708306
| Common name |
Hepta-tert-butyl-nonaphosphine(7) |
| Chemical name |
'1,3,3',4,4',5,5'-Hepta-tert-butyl-nonaphosphine(7)' |
| Formula |
C28 H63 P9 |
| Calculated formula |
C28 H63 P9 |
| Title of publication |
Facile synthesis of cyclo-(P4tBu3)-containing oligo- and pnictaphosphanes |
| Authors of publication |
Eilrich, Volker Jens; Grell, Toni; Lönnecke, Peter; Hey-Hawkins, Evamarie |
| Journal of publication |
Dalton Transactions |
| Year of publication |
2021 |
| a |
9.8283 ± 0.0002 Å |
| b |
13.4869 ± 0.0003 Å |
| c |
15.1621 ± 0.0003 Å |
| α |
84.231 ± 0.002° |
| β |
82.229 ± 0.002° |
| γ |
77.488 ± 0.002° |
| Cell volume |
1938.76 ± 0.07 Å3 |
| Cell temperature |
130 ± 2 K |
| Ambient diffraction temperature |
130 ± 2 K |
| Number of distinct elements |
3 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0316 |
| Residual factor for significantly intense reflections |
0.0245 |
| Weighted residual factors for significantly intense reflections |
0.059 |
| Weighted residual factors for all reflections included in the refinement |
0.0623 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.062 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7708306.html
