Crystallography Open Database

Information card for entry 7708309

Preview

Coordinates	7708309.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H51 Li N2 O P4
Calculated formula	C22 H51 Li N2 O P4
Title of publication	Facile synthesis of cyclo-(P4tBu3)-containing oligo- and pnictaphosphanes
Authors of publication	Eilrich, Volker Jens; Grell, Toni; Lönnecke, Peter; Hey-Hawkins, Evamarie
Journal of publication	Dalton Transactions
Year of publication	2021
a	8.8751 ± 0.0002 Å
b	15.4665 ± 0.0003 Å
c	11.1923 ± 0.0003 Å
α	90°
β	105.434 ± 0.003°
γ	90°
Cell volume	1480.93 ± 0.06 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0491
Residual factor for significantly intense reflections	0.0384
Weighted residual factors for significantly intense reflections	0.0798
Weighted residual factors for all reflections included in the refinement	0.0861
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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