Information card for entry 7708644

Structure parameters

• Formula: C27 H32 K P S2
• Calculated formula: C27 H32 K P S2
• Title of publication: On the Reaction of Potassium Phosphide KP(iPr)Ter with Chalcogenes, Heteroallenes and Acyl Chloride
• Authors of publication: Schulz, Axel; Szych, Lilian; Pilopp, Yannic; Bresien, Jonas; Villinger, Alexander; Lüdtke, Karsten Paul
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 8.0832 ± 0.0009 Å
• b: 11.7679 ± 0.0014 Å
• c: 14.3637 ± 0.0016 Å
• α: 86.631 ± 0.004°
• β: 81.445 ± 0.004°
• γ: 74.285 ± 0.004°
• Cell volume: 1300.4 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0531
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0896
• Weighted residual factors for all reflections included in the refinement: 0.1006
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No