Information card for entry 7708678
Formula |
C30 H47 Fe P3 Si |
Calculated formula |
C30 H47 Fe P3 Si |
Title of publication |
Synthesis of Silyl Iron Dinitrogen Complexes for Activation of Dihydrogen and Catalytic Silylation of Dinitrogen |
Authors of publication |
Chang, Guoliang; Zhang, Peng; Yang, Wenjing; Dong, Yanhong; Xie, Shangqing; Sun, Hongjian; Li, Xiaoyan; Fuhr, Olaf; Fenske, Dieter |
Journal of publication |
Dalton Transactions |
Year of publication |
2021 |
a |
9.1689 ± 0.0002 Å |
b |
16.6564 ± 0.0003 Å |
c |
21.0278 ± 0.0005 Å |
α |
90° |
β |
101.511 ± 0.002° |
γ |
90° |
Cell volume |
3146.79 ± 0.12 Å3 |
Cell temperature |
180 K |
Ambient diffraction temperature |
180 K |
Number of distinct elements |
5 |
Space group number |
14 |
Hermann-Mauguin space group symbol |
P 1 21/n 1 |
Hall space group symbol |
-P 2yn |
Residual factor for all reflections |
0.029 |
Residual factor for significantly intense reflections |
0.027 |
Weighted residual factors for significantly intense reflections |
0.0741 |
Weighted residual factors for all reflections included in the refinement |
0.0754 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.026 |
Diffraction radiation probe |
x-ray |
Diffraction radiation wavelength |
1.34143 Å |
Diffraction radiation type |
GaKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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https://www.crystallography.net/7708678.html