Information card for entry 7708734

Structure parameters

• Formula: C45 H93 N Si11
• Calculated formula: C45.04 H93.04 N Si11
• Title of publication: Silole Allylic Anions Instead of Silanides
• Authors of publication: Pöcheim, Alexander; Albers, Lena; Müller, Thomas; Baumgartner, Judith; Marschner, Christoph
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 37.205 ± 0.01 Å
• b: 13.523 ± 0.003 Å
• c: 25.072 ± 0.006 Å
• α: 90°
• β: 96.287 ± 0.008°
• γ: 90°
• Cell volume: 12538 ± 5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1537
• Residual factor for significantly intense reflections: 0.1381
• Weighted residual factors for significantly intense reflections: 0.2682
• Weighted residual factors for all reflections included in the refinement: 0.2779
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No