Information card for entry 7708802
| Formula |
C54.71 H66.43 B9 Cl1.71 O Os P4 Pt |
| Calculated formula |
C54.712 H66.424 B9 Cl1.712 O Os P4 Pt |
| Title of publication |
A simple and high-yield route to iridium, rhodium, osmium and ruthenium nido-6-metalladecaborane compounds |
| Authors of publication |
Bould, Jonathan; Londesborough, Michael G. S.; Passarelli, Vincenzo; Clegg, William; Waddell, Paul G.; Cvačka, Josef; Macías, Ramón |
| Journal of publication |
Dalton Transactions |
| Year of publication |
2021 |
| a |
9.7993 ± 0.0002 Å |
| b |
13.3272 ± 0.0002 Å |
| c |
22.1505 ± 0.0004 Å |
| α |
82.1298 ± 0.0014° |
| β |
81.7826 ± 0.0015° |
| γ |
87.9309 ± 0.0015° |
| Cell volume |
2835.72 ± 0.09 Å3 |
| Cell temperature |
150 ± 2 K |
| Ambient diffraction temperature |
150 ± 2 K |
| Number of distinct elements |
8 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0206 |
| Residual factor for significantly intense reflections |
0.0182 |
| Weighted residual factors for significantly intense reflections |
0.042 |
| Weighted residual factors for all reflections included in the refinement |
0.043 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.079 |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/7708802.html
