Information card for entry 7708861

Structure parameters

• Formula: C52.6 H65.2 Cl1.2 F40 Ge4 O36 P8 S12
• Calculated formula: C52.6 H65.2 Cl1.2 F40 Ge4 O36 P8 S12
• Title of publication: Neutral and cationic germanium(IV) fluoride complexes with phosphine coordination – synthesis, spectroscopy and structures
• Authors of publication: King, Rhys; Levason, William; Reid, Gillian
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 17.7401 ± 0.0002 Å
• b: 9.0881 ± 0.0001 Å
• c: 33.673 ± 0.0003 Å
• α: 90°
• β: 100.215 ± 0.001°
• γ: 90°
• Cell volume: 5342.84 ± 0.1 ų
• Cell temperature: 100.1 ± 0.4 K
• Ambient diffraction temperature: 100.1 ± 0.4 K
• Number of distinct elements: 8
• Space group number: 5
• Hermann-Mauguin space group symbol: I 1 2 1
• Hall space group symbol: I 2y
• Residual factor for all reflections: 0.0377
• Residual factor for significantly intense reflections: 0.0321
• Weighted residual factors for significantly intense reflections: 0.0657
• Weighted residual factors for all reflections included in the refinement: 0.0681
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No