Information card for entry 7708863

Structure parameters

• Formula: C24 H54 F24 Ge3 O18 P6 S6
• Calculated formula: C24 H54 F24 Ge3 O18 P6 S6
• Title of publication: Neutral and cationic germanium(IV) fluoride complexes with phosphine coordination – synthesis, spectroscopy and structures
• Authors of publication: King, Rhys; Levason, William; Reid, Gillian
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 9.3701 ± 0.0003 Å
• b: 15.5931 ± 0.0006 Å
• c: 21.5703 ± 0.0007 Å
• α: 93.05 ± 0.003°
• β: 94.382 ± 0.003°
• γ: 91.974 ± 0.003°
• Cell volume: 3135.6 ± 0.19 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1134
• Residual factor for significantly intense reflections: 0.0709
• Weighted residual factors for significantly intense reflections: 0.1898
• Weighted residual factors for all reflections included in the refinement: 0.2168
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0256
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No