Information card for entry 7709114

Structure parameters

• Formula: C44 H45 Cl4 N7 O0.5 Pd2
• Calculated formula: C44 H45 Cl4 N7 O0.5 Pd2
• Title of publication: Shape-selective one-step synthesis of branched gold nanoparticles on the crystal surface of redox-active Pd^II-macrocycles.
• Authors of publication: Yamashita, Yutaro; Tashiro, Shohei; Ishii, Yoshiki; Uchihashi, Takayuki; Matsushita, Nobuyuki; Kubota, Ryou; Shionoya, Mitsuhiko
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2022
• Journal volume: 51
• Journal issue: 4
• Pages of publication: 1318 - 1324
• a: 13.2066 ± 0.0002 Å
• b: 23.2676 ± 0.0004 Å
• c: 14.0442 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4315.58 ± 0.14 ų
• Cell temperature: 93 K
• Ambient diffraction temperature: 93 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0783
• Residual factor for significantly intense reflections: 0.0685
• Weighted residual factors for significantly intense reflections: 0.2022
• Weighted residual factors for all reflections included in the refinement: 0.2127
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No