Information card for entry 7709174

Structure parameters

• Formula: C61 H132 Fe K2 N5 O4 P Si6
• Calculated formula: C61 H132 Fe K2 N5 O4 P Si6
• Title of publication: Synthesis of the open-shell 3d-transition metal(II) bis(phosphinidenide) [Mn{P(sIDipp)}₂].
• Authors of publication: Weller, Ruth; Balmer, Markus; Hänisch, Carsten von; Gunnar Werncke, C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2022
• Journal volume: 51
• Journal issue: 5
• Pages of publication: 1765 - 1768
• a: 16.989 ± 0.0017 Å
• b: 26.471 ± 0.003 Å
• c: 18.6846 ± 0.0019 Å
• α: 90°
• β: 103.571 ± 0.008°
• γ: 90°
• Cell volume: 8168.2 ± 1.5 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1261
• Residual factor for significantly intense reflections: 0.059
• Weighted residual factors for significantly intense reflections: 0.1338
• Weighted residual factors for all reflections included in the refinement: 0.1525
• Goodness-of-fit parameter for all reflections included in the refinement: 0.896
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No