Information card for entry 7709202

Structure parameters

• Formula: C68 H50 Cl3 Cr N8 O10 Os3 Sn
• Calculated formula: C68 H50 Cl3 Cr N8 O10 Os3 Sn
• Title of publication: Complexes of transition metal carbonyl clusters with tin(II) phthalocyanine in neutral and radical anion states: methods of synthesis, structures and properties
• Authors of publication: Romanenko, Nikita R.; Kuzmin, Alexey V.; Khasanov, Salavat S.; Faraonov, Maxim A.; Yudanova, Evgeniya I.; Nakano, Yoshiaki; Otsuka, Akihiro; Yamochi, Hideki; Kitagawa, Hiroshi; Konarev, Dmitri V.
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 16.8961 ± 0.0004 Å
• b: 20.0969 ± 0.0004 Å
• c: 19.6999 ± 0.0004 Å
• α: 90°
• β: 96.102 ± 0.002°
• γ: 90°
• Cell volume: 6651.4 ± 0.2 ų
• Cell temperature: 130 ± 4 K
• Ambient diffraction temperature: 130 ± 4 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0511
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.1092
• Weighted residual factors for all reflections included in the refinement: 0.113
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No