Information card for entry 7709213

Structure parameters

• Formula: C35 H35 N2 O9 P Ru3
• Calculated formula: C35 H35 N2 O9 P Ru3
• Title of publication: Synthesis, molecular structure and fluxional behavior of the elusive [HRu4(CO)12]3– carbonyl anion
• Authors of publication: Cesari, Cristiana; Bortoluzzi, Marco; Femoni, Cristina; Iapalucci, Maria Carmela; Zacchini, Stefano
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 11.1727 ± 0.0011 Å
• b: 11.9062 ± 0.0012 Å
• c: 14.3383 ± 0.0014 Å
• α: 90.095 ± 0.003°
• β: 99.075 ± 0.003°
• γ: 100.292 ± 0.003°
• Cell volume: 1852.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0622
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.0964
• Weighted residual factors for all reflections included in the refinement: 0.0993
• Goodness-of-fit parameter for all reflections included in the refinement: 1.172
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No