Information card for entry 7709260

Structure parameters

• Formula: C57 H42 B F20 N S Si
• Calculated formula: C57 H42 B F20 N S Si
• Title of publication: Norbornene based-sulfide-stabilized silylium ions: synthesis, structure and application in catalysis.
• Authors of publication: Dajnak, Aymeric; Özpınar, Gül Altınbaş; Lenk, Romaric; Saffon-Merceron, Nathalie; Baceiredo, Antoine; Kato, Tsuyoshi; Müller, Thomas; Maerten, Eddy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2022
• Journal volume: 51
• Journal issue: 4
• Pages of publication: 1407 - 1414
• a: 12.7325 ± 0.0008 Å
• b: 13.4053 ± 0.0009 Å
• c: 16.4281 ± 0.001 Å
• α: 85.829 ± 0.002°
• β: 69.6571 ± 0.0017°
• γ: 89.197 ± 0.0019°
• Cell volume: 2622 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0939
• Residual factor for significantly intense reflections: 0.0507
• Weighted residual factors for significantly intense reflections: 0.1057
• Weighted residual factors for all reflections included in the refinement: 0.1242
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No