Information card for entry 7709324

Structure parameters

• Formula: C2 H3 Cl4 N Se W
• Calculated formula: C2 H3 Cl4 N Se W
• Title of publication: Tungsten(vi) selenide tetrachloride, WSeCl4 – synthesis, properties, coordination complexes and application of [WSeCl4(SenBu2)] for CVD growth of WSe2 thin films
• Authors of publication: Greenacre, Victoria K.; Hector, Andrew L.; Huang, Ruomeng; Levason, William; Sethi, Vikesh; Reid, Gillian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 5.8784 ± 0.0002 Å
• b: 7.8378 ± 0.0004 Å
• c: 14.814 ± 0.0006 Å
• α: 90°
• β: 88.834 ± 0.003°
• γ: 90°
• Cell volume: 682.39 ± 0.05 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0459
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.1029
• Weighted residual factors for all reflections included in the refinement: 0.1089
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No