Information card for entry 7709334

Structure parameters

• Chemical name: (Z)-2,2-dimethyl-1-((triphenylsilyl)oxy)propylidene)(triphenylsilyl)
• Formula: C10.25 H9.75 O0.25 P0.25 Si0.5
• Calculated formula: C10.25 H9.75 O0.25 P0.25 Si0.5
• Title of publication: Simple conversion of trisodium phosphide, Na3P, into silyl- and cyanophosphides and structure of a terminal silver phosphide
• Authors of publication: Grützmacher, Hansjörg; Le Corre, Grégoire
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 23.112 ± 0.002 Å
• b: 13.4449 ± 0.0012 Å
• c: 11.1997 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3480.2 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0363
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0799
• Weighted residual factors for all reflections included in the refinement: 0.0852
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No