Information card for entry 7709356

Structure parameters

• Formula: C97 H152 Cl Li N9 O7 Si6 Y3
• Calculated formula: C97 H152 Cl Li N9 O7 Si6 Y3
• Title of publication: Synthesis and characterization of rare-earth metallate amido complexes bearing 2-amidate-functionalized indolyl ligand and their application in the hydroboration of esters with pinacolborane
• Authors of publication: Wei, Yun; Bao, Qin; Song, Lulu; Hong, Dongjing; Gao, Jianjian; Wang, Shaowu; Zhu, Xiancui; Zhou, Shuangliu; Mu, Xiaolong
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 19.816 ± 0.002 Å
• b: 20.172 ± 0.002 Å
• c: 21.517 ± 0.002 Å
• α: 67.643 ± 0.001°
• β: 83.979 ± 0.002°
• γ: 61.661 ± 0.001°
• Cell volume: 6970.8 ± 1.2 ų
• Cell temperature: 298.15 K
• Ambient diffraction temperature: 298.15 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1939
• Residual factor for significantly intense reflections: 0.0774
• Weighted residual factors for significantly intense reflections: 0.1811
• Weighted residual factors for all reflections included in the refinement: 0.2275
• Goodness-of-fit parameter for all reflections included in the refinement: 0.956
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No