Information card for entry 7709478

Structure parameters

• Formula: Al5 Cl22 S16 Sb13
• Calculated formula: Al5 Cl22 S16 Sb13
• Title of publication: Exploration of metal sulfide syntheses and the dissolution process of antimony sulfide in phosphonium-based ionic liquids.
• Authors of publication: Grasser, Matthias A.; Pietsch, Tobias; Brunner, Eike; Ruck, Michael
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2022
• Journal volume: 51
• Journal issue: 10
• Pages of publication: 4079 - 4086
• a: 8.8886 ± 0.001 Å
• b: 19.043 ± 0.002 Å
• c: 21.125 ± 0.002 Å
• α: 63.884 ± 0.002°
• β: 80.322 ± 0.002°
• γ: 88.699 ± 0.002°
• Cell volume: 3159.7 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for significantly intense reflections: 0.0265
• Weighted residual factors for all reflections included in the refinement: 0.0273
• Goodness-of-fit parameter for all reflections included in the refinement: 1.308
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No