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Information card for entry 7709481
Preview
Coordinates | 7709481.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C57 H68 B F40 P2 Rh S8 |
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Calculated formula | C57 H68 B F40 P2 Rh S8 |
Title of publication | MicroED characterization of a robust cationic σ-alkane complex stabilized by the [B(3,5-(SF5)2C6H3)4]− anion, via on-grid solid/gas single-crystal to single-crystal reactivity |
Authors of publication | Doyle, Laurence R.; Thompson, Emily A.; Burnage, Arron L.; Whitwood, Adrian C.; Jenkins, Huw T.; Macgregor, Stuart A.; Weller, Andrew S. |
Journal of publication | Dalton Transactions |
Year of publication | 2022 |
a | 19.603 ± 0.003 Å |
b | 18.393 ± 0.003 Å |
c | 20.438 ± 0.002 Å |
α | 90° |
β | 92.355 ± 0.012° |
γ | 90° |
Cell volume | 7362.9 ± 1.8 Å3 |
Cell temperature | 80 ± 2 K |
Ambient diffraction temperature | 80 ± 2 K |
Number of distinct elements | 7 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.2194 |
Residual factor for significantly intense reflections | 0.1565 |
Weighted residual factors for significantly intense reflections | 0.3421 |
Weighted residual factors for all reflections included in the refinement | 0.3584 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.718 |
Diffraction radiation probe | electron |
Diffraction radiation wavelength | 0.02508 Å |
Diffraction radiation type | electron |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7709481.html
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