Information card for entry 7709572

Structure parameters

• Formula: C38 H94 Cl2 Fe2 N4 Si6
• Calculated formula: C38 H94 Cl2 Fe2 N4 Si6
• Title of publication: Trisyl-based multidentate ligands: synthesis and their transition-metal complexes
• Authors of publication: Yin, Zhu-Bao; Wei, Junnian; Xi, Zhenfeng
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 9.0648 ± 0.0005 Å
• b: 12.2798 ± 0.0007 Å
• c: 12.6473 ± 0.0007 Å
• α: 100.964 ± 0.005°
• β: 92.641 ± 0.004°
• γ: 99.343 ± 0.005°
• Cell volume: 1359.48 ± 0.14 ų
• Cell temperature: 179.99 ± 0.1 K
• Ambient diffraction temperature: 179.99 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0612
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for significantly intense reflections: 0.085
• Weighted residual factors for all reflections included in the refinement: 0.0918
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No