Information card for entry 7709575

Structure parameters

• Formula: C19 H47 Li N2 Si3
• Calculated formula: C19 H47 Li N2 Si3
• Title of publication: Trisyl-based multidentate ligands: synthesis and their transition-metal complexes
• Authors of publication: Yin, Zhu-Bao; Wei, Junnian; Xi, Zhenfeng
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 15.81 ± 0.0009 Å
• b: 10.4149 ± 0.0004 Å
• c: 16.2663 ± 0.0009 Å
• α: 90°
• β: 108.524 ± 0.006°
• γ: 90°
• Cell volume: 2539.6 ± 0.2 ų
• Cell temperature: 180 ± 0.1 K
• Ambient diffraction temperature: 180 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0471
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0939
• Weighted residual factors for all reflections included in the refinement: 0.0993
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No