Information card for entry 7709653

Structure parameters

• Formula: C56 H72 B3 F24 O4 P4 Rh
• Calculated formula: C56 H72 B3 F24 O4 P4 Rh
• Title of publication: Ligand properties of boryl ligands in bis-boryl rhodium(iii) complexes: a case study
• Authors of publication: Drescher, Wiebke; Kleeberg, Christian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 21.7869 ± 0.0007 Å
• b: 13.4146 ± 0.0003 Å
• c: 24.8701 ± 0.0008 Å
• α: 90°
• β: 113.69 ± 0.004°
• γ: 90°
• Cell volume: 6656.1 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0728
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.1274
• Weighted residual factors for all reflections included in the refinement: 0.1323
• Goodness-of-fit parameter for all reflections included in the refinement: 1.129
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No