Information card for entry 7709658

Structure parameters

• Formula: C54.5 H59.2 B2 Cl8 O4 P2 Rh
• Calculated formula: C51 H51 B2 Cl7 O4 P2 Rh
• Title of publication: Ligand properties of boryl ligands in bis-boryl rhodium(iii) complexes: a case study
• Authors of publication: Drescher, Wiebke; Kleeberg, Christian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 11.2915 ± 0.0002 Å
• b: 21.8994 ± 0.0004 Å
• c: 23.4243 ± 0.0005 Å
• α: 90°
• β: 95.632 ± 0.002°
• γ: 90°
• Cell volume: 5764.33 ± 0.19 ų
• Cell temperature: 102 ± 2 K
• Ambient diffraction temperature: 102 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0471
• Residual factor for significantly intense reflections: 0.0375
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.0839
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No