Information card for entry 7710107

Structure parameters

• Formula: C212 H252 Cl4 F24 Ir4 N16 O3 P12 Si4
• Calculated formula: C212 H252 Cl4 F24 Ir4 N16 O3 P12 Si4
• Title of publication: Synthesis and reactivity of an iridium complex based on a tridentate aminophosphano ligand
• Authors of publication: Palmese, Marco; Pérez-Torrente, Jesús J.; Passarelli, Vincenzo
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 46.824 ± 0.005 Å
• b: 10.9773 ± 0.0011 Å
• c: 25.668 ± 0.003 Å
• α: 90°
• β: 121.193 ± 0.001°
• γ: 90°
• Cell volume: 11286 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0364
• Weighted residual factors for significantly intense reflections: 0.0738
• Weighted residual factors for all reflections included in the refinement: 0.0815
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No