Crystallography Open Database

Information card for entry 7710114

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Coordinates	7710114.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H48 O0.5 P3 Pd Zn
Calculated formula	C56 H48 O0.5 P3 Pd Zn
Title of publication	Facile Synthesis and Utilization of Bis(o-phosphinophenyl)zinc as Isolable PZnP-pincer Ligands Enabled by Boron-Zinc Double Transmetallation
Authors of publication	Fukuda, Kazuishi; Harada, Takuma; Iwasawa, Nobuharu; Takaya, Jun
Journal of publication	Dalton Transactions
Year of publication	2022
a	9.1351 ± 0.0002 Å
b	13.0286 ± 0.0003 Å
c	20.1713 ± 0.0006 Å
α	93.909 ± 0.002°
β	97.565 ± 0.002°
γ	96.028 ± 0.002°
Cell volume	2358.48 ± 0.1 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0393
Residual factor for significantly intense reflections	0.0333
Weighted residual factors for significantly intense reflections	0.0826
Weighted residual factors for all reflections included in the refinement	0.0851
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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