Information card for entry 7710147

Structure parameters

• Formula: C120 H164 Ge4 N8 O2
• Calculated formula: C120 H164 Ge4 N8 O2
• Title of publication: An α-diiminato germylene family: syntheses, structures, and reactivity towards C-C coupled digermylene and digermylene oxide
• Authors of publication: Liu, Jingjing; Shang, Jianxuan; Wei, Jing; Gao, Fangfang; Hou, Lei; Zeng, FanLong; Li, Anyang; Wang, Wenyuan
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 13.4853 ± 0.0005 Å
• b: 24.7376 ± 0.0013 Å
• c: 34.1042 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11377 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0441
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0909
• Weighted residual factors for all reflections included in the refinement: 0.095
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 1.34138 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No