Information card for entry 7710273

Structure parameters

• Formula: C45 H53 Mg N O2
• Calculated formula: C45 H53 Mg N O2
• Title of publication: Sterically shielded primary anilides of the alkaline-earth metals of the type (thf)nAe(NH-Ar*)2 (Ae = Mg, Ca, Sr, and Ba; Ar* = bulky aryl)
• Authors of publication: Westerhausen, Matthias; Schüler, Philipp; Krieck, Sven; Görls, Helmar; Liebing, Phil
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 27.9665 ± 0.0005 Å
• b: 17.3376 ± 0.0004 Å
• c: 18.954 ± 0.0005 Å
• α: 90°
• β: 124.62 ± 0.001°
• γ: 90°
• Cell volume: 7563 ± 0.3 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1228
• Residual factor for significantly intense reflections: 0.0884
• Weighted residual factors for significantly intense reflections: 0.1939
• Weighted residual factors for all reflections included in the refinement: 0.2154
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No