Information card for entry 7710304

Structure parameters

• Formula: C24 H33 N5 O21 W5 Zn
• Calculated formula: C24 H33 N5 O21 W5 Zn
• Title of publication: Merging of the photocatalyst decatungstate and naphthalene diimide in a hybrid structure for the oxidative coupling of amines
• Authors of publication: Liu, Zhengfen; Li, Xiaobo; Chen, Jian; Li, Chao; Luo, Fumang; Cheng, Fei-Xiang; Liu, Jian-Jun
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 11.6641 ± 0.0006 Å
• b: 12.288 ± 0.0006 Å
• c: 17.5529 ± 0.0006 Å
• α: 104.503 ± 0.004°
• β: 102.541 ± 0.004°
• γ: 105.931 ± 0.004°
• Cell volume: 2229 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.045
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0932
• Weighted residual factors for all reflections included in the refinement: 0.0972
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No