Information card for entry 7710416

Structure parameters

• Formula: K5 Na O24 S6 Sm2
• Calculated formula: K5 Na O24 S6 Sm2
• Title of publication: Delicate, a study of the structural changes in ten-coordinated La(iii), Ce(iii), Pr(iii), Nd(iii), Sm(iii) and Eu(iii) sulfates
• Authors of publication: Storm Thomsen, Maria; Sørensen, Thomas Just
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 9.1152 ± 0.0006 Å
• b: 16.1688 ± 0.001 Å
• c: 7.6393 ± 0.0004 Å
• α: 90°
• β: 110.639 ± 0.002°
• γ: 90°
• Cell volume: 1053.63 ± 0.11 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.019
• Residual factor for significantly intense reflections: 0.0168
• Weighted residual factors for significantly intense reflections: 0.0436
• Weighted residual factors for all reflections included in the refinement: 0.0443
• Goodness-of-fit parameter for all reflections included in the refinement: 1.12
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No