Information card for entry 7710529

Structure parameters

• Formula: C30 H39 O P
• Calculated formula: C30 H39 O P
• Title of publication: Modulating the reactivity of phosphanylidenephosphoranes towards water with Lewis acids
• Authors of publication: Dankert, Fabian; Fischer, Malte; Hering-Junghans, Christian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 12.2456 ± 0.0002 Å
• b: 16.9887 ± 0.0003 Å
• c: 13.3272 ± 0.0002 Å
• α: 90°
• β: 100.383 ± 0.0008°
• γ: 90°
• Cell volume: 2727.15 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0581
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.1221
• Weighted residual factors for all reflections included in the refinement: 0.1318
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No