Information card for entry 7710746
Formula |
C155 H242 Br4 N2 Ni2 O56 P2 |
Calculated formula |
C155 H242 Br4 N2 Ni2 O56 P2 |
Title of publication |
A cavity-shaped <i>cis</i>-chelating P,N ligand for highly selective nickel-catalysed ethylene dimerisation. |
Authors of publication |
Li, Yang; Pelzer, Katrin; Sechet, Damien; Creste, Geordie; Matt, Dominique; Braunstein, Pierre; Armspach, Dominique |
Journal of publication |
Dalton transactions (Cambridge, England : 2003) |
Year of publication |
2022 |
a |
17.8671 ± 0.0006 Å |
b |
17.8671 ± 0.0006 Å |
c |
53.805 ± 0.002 Å |
α |
90° |
β |
90° |
γ |
90° |
Cell volume |
17176.3 ± 1 Å3 |
Cell temperature |
120 ± 2 K |
Ambient diffraction temperature |
120 ± 2 K |
Number of distinct elements |
7 |
Space group number |
92 |
Hermann-Mauguin space group symbol |
P 41 21 2 |
Hall space group symbol |
P 4abw 2nw |
Residual factor for all reflections |
0.0741 |
Residual factor for significantly intense reflections |
0.0515 |
Weighted residual factors for significantly intense reflections |
0.1343 |
Weighted residual factors for all reflections included in the refinement |
0.1474 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.04 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
Yes |
Has Fobs |
No |
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https://www.crystallography.net/7710746.html