Information card for entry 7710761

Structure parameters

• Formula: C32 H63 F6 O2 P3 Pd
• Calculated formula: C32 H63 F6 O2 P3 Pd
• Title of publication: Heterolytic carbon–iodine bond cleavage by a palladium(i) metalloradical
• Authors of publication: Sinclair, Matthew J. G.; Chaplin, Adrian B.
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 14.7315 ± 0.0003 Å
• b: 15.354 ± 0.0003 Å
• c: 16.2276 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3670.48 ± 0.12 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0872
• Residual factor for significantly intense reflections: 0.0834
• Weighted residual factors for significantly intense reflections: 0.186
• Weighted residual factors for all reflections included in the refinement: 0.1873
• Goodness-of-fit parameter for all reflections included in the refinement: 1.436
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No