Information card for entry 7710920

Structure parameters

• Formula: C52 H104 Al2 Si10
• Calculated formula: C52 H104 Al2 Si10
• Title of publication: Synthesis of bi- and tetradentate poly-Lewis acids by hydroalumination of poly-alkynyl-anthracene derivatives
• Authors of publication: Mitzel, Norbert Werner; Aders, Niklas; Lamm, Jan-Hendrik; Beckmann, Jean Louis; Neumann, Beate; Stammler, Georg
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 17.90519 ± 0.00019 Å
• b: 10.80972 ± 0.00012 Å
• c: 35.6601 ± 0.0005 Å
• α: 90°
• β: 98.7252 ± 0.0012°
• γ: 90°
• Cell volume: 6822.14 ± 0.14 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.036
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0808
• Weighted residual factors for all reflections included in the refinement: 0.0847
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No