Information card for entry 7710926

Structure parameters

• Formula: C160 H244 Al4 N4 Si16
• Calculated formula: C160 H244 Al4 N4 Si16
• Title of publication: Synthesis of bi- and tetradentate poly-Lewis acids by hydroalumination of poly-alkynyl-anthracene derivatives
• Authors of publication: Mitzel, Norbert Werner; Aders, Niklas; Lamm, Jan-Hendrik; Beckmann, Jean Louis; Neumann, Beate; Stammler, Georg
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 15.7845 ± 0.0003 Å
• b: 22.9127 ± 0.0005 Å
• c: 26.7425 ± 0.0005 Å
• α: 111.11 ± 0.002°
• β: 103.729 ± 0.002°
• γ: 96.176 ± 0.002°
• Cell volume: 8563.8 ± 0.3 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.092
• Residual factor for significantly intense reflections: 0.0632
• Weighted residual factors for significantly intense reflections: 0.1698
• Weighted residual factors for all reflections included in the refinement: 0.1856
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No