Information card for entry 7710939

Structure parameters

• Formula: C28 H42 N14 O16 Pd2
• Calculated formula: C28 H42 N14 O16 Pd2
• Title of publication: Diastereoselectively self-sorted low-symmetry binuclear metallomacrocycle and trinuclear metallocage.
• Authors of publication: Mishra, Srabani Srotoswini; Chand, Dillip Kumar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2022
• Journal volume: 51
• Journal issue: 31
• Pages of publication: 11650 - 11657
• a: 7.7499 ± 0.0009 Å
• b: 10.4043 ± 0.0012 Å
• c: 12.9225 ± 0.0015 Å
• α: 87.015 ± 0.005°
• β: 74.757 ± 0.005°
• γ: 75.488 ± 0.005°
• Cell volume: 973.1 ± 0.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1082
• Residual factor for significantly intense reflections: 0.099
• Weighted residual factors for significantly intense reflections: 0.286
• Weighted residual factors for all reflections included in the refinement: 0.3024
• Goodness-of-fit parameter for all reflections included in the refinement: 1.257
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No