Information card for entry 7710959

Structure parameters

• Formula: C18 H32 O2 P2
• Calculated formula: C18 H32 O2 P2
• Title of publication: Substitution of Hyp (Hyp = Si(SiMe3)3) at metalloid [Ge9(Hyp)3]- clusters using phosphine stabilized Au(I)Cl.
• Authors of publication: Schnepf, Andreas; Gienger, Christian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 5.6229 ± 0.0012 Å
• b: 7.5296 ± 0.0016 Å
• c: 11.956 ± 0.003 Å
• α: 85.464 ± 0.003°
• β: 80.159 ± 0.003°
• γ: 79.593 ± 0.003°
• Cell volume: 489.94 ± 0.19 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0372
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.0818
• Weighted residual factors for all reflections included in the refinement: 0.0858
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No