Information card for entry 7710967

Structure parameters

• Formula: C20 H31 I2 N Pb
• Calculated formula: C20 H31 I2 N Pb
• Title of publication: N-Heterocyclic Carbene and Cyclic (Alkyl)(amino)carbene Adducts of Plumbanes and Plumbylenes
• Authors of publication: Radius, Udo; Philipp, Michael S. M.; Bertermann, Rüdiger
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 11.1728 ± 0.0002 Å
• b: 10.3375 ± 0.0001 Å
• c: 20.4224 ± 0.0003 Å
• α: 90°
• β: 101.047 ± 0.001°
• γ: 90°
• Cell volume: 2315.06 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0148
• Residual factor for significantly intense reflections: 0.0138
• Weighted residual factors for significantly intense reflections: 0.0339
• Weighted residual factors for all reflections included in the refinement: 0.0342
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No