Information card for entry 7711020

Structure parameters

• Formula: C23 H39 I N Si U
• Calculated formula: C23 H39 I N Si U
• Title of publication: Identification of the U(v) complex (C5Me5)2UVI(NSiMe3) in the reaction of (C5Me5)2UIIII(THF) with N3SiMe3
• Authors of publication: Wedal, Justin C.; Ziller, Joseph W.; Evans, William J.
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 10.0187 ± 0.0012 Å
• b: 15.8538 ± 0.0019 Å
• c: 19.991 ± 0.002 Å
• α: 90°
• β: 101.629 ± 0.0018°
• γ: 90°
• Cell volume: 3110.1 ± 0.6 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0911
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for significantly intense reflections: 0.1616
• Weighted residual factors for all reflections included in the refinement: 0.1737
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No